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Information card for entry 7238607
Preview
Coordinates | 7238607.cif |
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Original paper (by DOI) | HTML |
Formula | C67 H57 Cl N5 O3 P3 Pd Ru |
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Calculated formula | C67 H57 Cl N5 O3 P3 Pd Ru |
Title of publication | Mononuclear palladium and heterodinuclear palladium‒ruthenium complexes of semicarbazone ligands. Synthesis, characterization, and application in C‒C cross-coupling reactions |
Authors of publication | Datta, Sayanti; Kumar Seth, Dipravath; Halder, Sarmistha; Sheldrick, William S.; Mayer-Figge, Heike; Drew, Michael G. B.; Bhattacharya, Samaresh |
Journal of publication | RSC Advances |
Year of publication | 2012 |
Journal volume | 2 |
Journal issue | 12 |
Pages of publication | 5254 |
a | 10.2779 ± 0.0002 Å |
b | 13.7689 ± 0.0002 Å |
c | 22.0341 ± 0.0003 Å |
α | 99.315 ± 0.001° |
β | 103.302 ± 0.001° |
γ | 100.393 ± 0.001° |
Cell volume | 2916.58 ± 0.08 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0661 |
Residual factor for significantly intense reflections | 0.0415 |
Weighted residual factors for significantly intense reflections | 0.118 |
Weighted residual factors for all reflections included in the refinement | 0.1404 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.877 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7238607.html
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