Information card for entry 7238652

Structure parameters

• Formula: C30 H24 Cr O3 S3
• Calculated formula: C30 H24 Cr O3 S3
• Title of publication: Lithiation of η6-fluorobenzenetricarbonylchromium(0) and reaction with dialkyl disulfides: synthesis of η6-1,2-bis- and 1,2,3-tris-alkylsulfanylbenzenetricarbonylchromium(0) complexes
• Authors of publication: Woolford, Helen; Elsegood, Mark R. J.; Weaver, George W.
• Journal of publication: RSC Advances
• Year of publication: 2012
• Journal volume: 2
• Journal issue: 14
• Pages of publication: 6049
• a: 11.7886 ± 0.0007 Å
• b: 24.6453 ± 0.0015 Å
• c: 10.2118 ± 0.0006 Å
• α: 90°
• β: 115.625 ± 0.0009°
• γ: 90°
• Cell volume: 2675.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.103
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No