Information card for entry 7238667

Structure parameters

• Formula: C14 H19 N O
• Calculated formula: C14 H19 N O
• Title of publication: Waste reduction in amide synthesis by a continuous method based on recycling of the reaction mixture
• Authors of publication: Thalluri, Kishore; Nadimpally, Krishna Chaitanya; Paul, Ashim; Mandal, Bhubaneswar
• Journal of publication: RSC Advances
• Year of publication: 2012
• Journal volume: 2
• Journal issue: 17
• Pages of publication: 6838
• a: 9.493 ± 0.005 Å
• b: 11.707 ± 0.005 Å
• c: 12.816 ± 0.006 Å
• α: 79.59 ± 0.03°
• β: 73.54 ± 0.04°
• γ: 73.58 ± 0.03°
• Cell volume: 1302.4 ± 1.1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1314
• Residual factor for significantly intense reflections: 0.0672
• Weighted residual factors for significantly intense reflections: 0.1619
• Weighted residual factors for all reflections included in the refinement: 0.2003
• Goodness-of-fit parameter for all reflections included in the refinement: 0.908
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No