Crystallography Open Database

Information card for entry 7238684

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Coordinates	7238684.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H22 O
Calculated formula	C27 H22 O
Title of publication	A route to hydroxylfluorenes: TsOH-mediated condensation reactions of 1,3-diketones with propargylic alcohols
Authors of publication	Yao, Liang-Feng; Tan, Davin; Miao, Xiaohe; Huang, Kuo-Wei
Journal of publication	RSC Advances
Year of publication	2012
Journal volume	2
Journal issue	19
Pages of publication	7594
a	8.8927 ± 0.0007 Å
b	11.1096 ± 0.0009 Å
c	11.2148 ± 0.0007 Å
α	64.309 ± 0.007°
β	75.677 ± 0.006°
γ	87.598 ± 0.007°
Cell volume	964.68 ± 0.14 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0773
Residual factor for significantly intense reflections	0.0654
Weighted residual factors for significantly intense reflections	0.1939
Weighted residual factors for all reflections included in the refinement	0.2089
Goodness-of-fit parameter for all reflections included in the refinement	0.78
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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