Information card for entry 7238703

Structure parameters

• Formula: C19 H30 N2 O9
• Calculated formula: C19 H25 N2 O9
• Title of publication: Triphenylphosphine-mediated reaction of dialkyl azodicarboxylate with activated alkenes leading to pyrazolines
• Authors of publication: Yamazaki, Shoko; Maenaka, Yuta; Fujinami, Ken; Mikata, Yuji
• Journal of publication: RSC Advances
• Year of publication: 2012
• Journal volume: 2
• Journal issue: 21
• Pages of publication: 8095
• a: 9.2138 ± 0.0015 Å
• b: 9.2556 ± 0.0015 Å
• c: 14.723 ± 0.003 Å
• α: 99.6509 ± 0.0016°
• β: 96.6679 ± 0.0014°
• γ: 112.748 ± 0.0015°
• Cell volume: 1118.7 ± 0.3 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for all reflections included in the refinement: 0.1697
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No