Information card for entry 7238910

Structure parameters

• Formula: C18 H16 Br4 Cl Co N4 O6
• Calculated formula: C18 H16 Br4 Cl Co N4 O6
• Title of publication: A series of tetrabromocatecholate chelated cobalt(iii) complexes with various N-donor ancillary ligands: syntheses, crystal structures, co-crystallization, thermally induced valence tautomerism and electrochemical studies
• Authors of publication: Panja, Anangamohan
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 15
• Pages of publication: 4954
• a: 6.546 ± 0.002 Å
• b: 31.167 ± 0.011 Å
• c: 11.809 ± 0.003 Å
• α: 90°
• β: 104.774 ± 0.002°
• γ: 90°
• Cell volume: 2329.6 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for significantly intense reflections: 0.1402
• Weighted residual factors for all reflections included in the refinement: 0.1605
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No