Information card for entry 7238960

Structure parameters

• Formula: C21 H25 N O5 S
• Calculated formula: C21 H25 N O5 S
• Title of publication: l-Proline catalyzed highly efficient synthesis of Z-5-alkylidene cyclic sulfamidate imines: an easy access to 5-alkyl-substituted cyclic sulfamidate imines
• Authors of publication: Majee, Debashis; Srivastava, Anvita; Mobin, Shaikh M.; Samanta, Sampak
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 29
• Pages of publication: 11502
• a: 9.8446 ± 0.0003 Å
• b: 14.244 ± 0.0003 Å
• c: 15.0095 ± 0.0003 Å
• α: 90°
• β: 97.378 ± 0.002°
• γ: 90°
• Cell volume: 2087.3 ± 0.09 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.1062
• Weighted residual factors for all reflections included in the refinement: 0.1111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No