Crystallography Open Database

Information card for entry 7238979

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Coordinates	7238979.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H44 N2 O9
Calculated formula	C43 H44 N2 O9
Title of publication	Sequential Staudinger ketene‒imine cycloaddition, RCM approach to polycyclic macrocyclic bisazetidinones
Authors of publication	Ibrahim, Yehia A.; Al-Awadi, Nouria A.; Al-Azemi, Talal F.; Abraham, Susan; John, Elizabeth
Journal of publication	RSC Advances
Year of publication	2013
Journal volume	3
Journal issue	18
Pages of publication	6408
a	11.8216 ± 0.0004 Å
b	19.5371 ± 0.0006 Å
c	17.1819 ± 0.0012 Å
α	90°
β	108.392 ± 0.008°
γ	90°
Cell volume	3765.6 ± 0.4 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.0596
Weighted residual factors for all reflections included in the refinement	0.1841
Goodness-of-fit parameter for all reflections included in the refinement	1.095
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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