Information card for entry 7239124

Structure parameters

• Formula: C25 H104 N24 Ni5 O73 P2 W19
• Calculated formula: C25 H96 N24 Ni5 O73 P2 W19
• Title of publication: A polyoxometalate-based ionic crystal assembly from a heterometallic cluster and polyoxoanions with visible-light catalytic activity
• Authors of publication: Liu, Zhu-Jun; Yao, Shuang; Zhang, Zhi-Ming; Wang, En-Bo
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 43
• Pages of publication: 20829
• a: 21.4954 ± 0.0013 Å
• b: 21.4954 ± 0.0013 Å
• c: 21.4954 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9932 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 198
• Hermann-Mauguin space group symbol: P 21 3
• Hall space group symbol: P 2ac 2ab 3
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No