Information card for entry 7239233

Structure parameters

• Formula: C15 H14 N4 O2 S
• Calculated formula: C15 H14 N4 O2 S
• Title of publication: Ultrasound promoted catalyst-free and selective synthesis of spiro[indole-3,4′-pyrazolo[3,4-e][1,4]thiazepines] in aqueous media and evaluation of their anti-hyperglycemic activity
• Authors of publication: Dandia, Anshu; Singh, Ruby; Joshi, Jyoti; Maheshwari, Shuchi; Soni, Pragya
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 41
• Pages of publication: 18992
• a: 11.9823 ± 0.0006 Å
• b: 8.3551 ± 0.0004 Å
• c: 17.551 ± 0.0009 Å
• α: 90°
• β: 104.948 ± 0.002°
• γ: 90°
• Cell volume: 1697.63 ± 0.15 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0735
• Weighted residual factors for significantly intense reflections: 0.2496
• Weighted residual factors for all reflections included in the refinement: 0.2592
• Goodness-of-fit parameter for all reflections included in the refinement: 1.153
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No