Information card for entry 7239282

Structure parameters

• Formula: C18 H16 F N2 O2
• Calculated formula: C18 H16 F N2 O2
• Title of publication: A green approach for the one-pot multi-component synthesis of N-substituted γ, δ and ε-lactams involving C‒N bond formation catalyzed by FeCl3
• Authors of publication: Sathesh, Venkatesan; Sathishkumar, Munusamy; Ramachandran, Gunasekar; Rathore, Ravindranath S.; Sathiyanarayanan, Kulathu Iyer
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 45
• Pages of publication: 23035
• a: 8.2658 ± 0.0004 Å
• b: 15.6654 ± 0.0007 Å
• c: 12.7267 ± 0.0006 Å
• α: 90°
• β: 107.505 ± 0.002°
• γ: 90°
• Cell volume: 1571.63 ± 0.13 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0854
• Residual factor for significantly intense reflections: 0.0588
• Weighted residual factors for significantly intense reflections: 0.1738
• Weighted residual factors for all reflections included in the refinement: 0.2014
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No