Synthesis of 5,10,15,20-meso-unsubstituted and 5,10,15,20-meso-substituted-21,23-ditellura/diselena core-modified porphyrinogens: oxidation and detection of mercury(ii)
Authors of publication
Ahmad, Sohail; Yadav, Kumar Karitkey; Singh, Sarangthem Joychandra; Chauhan, S. M. S.
Journal of publication
RSC Adv.
Year of publication
2014
Journal volume
4
Journal issue
7
Pages of publication
3171
a
10.361 ± 0.002 Å
b
11.572 ± 0.003 Å
c
11.8258 ± 0.0015 Å
α
101.396 ± 0.015°
β
90.972 ± 0.013°
γ
104.51 ± 0.02°
Cell volume
1342.3 ± 0.5 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0848
Residual factor for significantly intense reflections
0.0713
Weighted residual factors for significantly intense reflections
0.1865
Weighted residual factors for all reflections included in the refinement
0.2017
Goodness-of-fit parameter for all reflections included in the refinement
