Information card for entry 7239788

Structure parameters

• Formula: C26 H38 F6 N16 O10
• Calculated formula: C26 H38 F6 N16 O10
• Title of publication: Efficient syntheses of macrocycles ranging from 22‒28 atoms through spontaneous dimerization to yield bis-hydrazones
• Authors of publication: Sharma, Vishal R.; Mehmood, Arshad; Janesko, Benjamin G.; Simanek, Eric E.
• Journal of publication: RSC Advances
• Year of publication: 2020
• Journal volume: 10
• Journal issue: 6
• Pages of publication: 3217 - 3220
• a: 9.5858 ± 0.0003 Å
• b: 18.8852 ± 0.0006 Å
• c: 10.9389 ± 0.0004 Å
• α: 90°
• β: 115.184 ± 0.001°
• γ: 90°
• Cell volume: 1792.03 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 99.96 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0631
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.1096
• Weighted residual factors for all reflections included in the refinement: 0.1179
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No