Information card for entry 7239792

Structure parameters

• Formula: C34 H56 F6 N16 O11
• Calculated formula: C34 H56 F6 N16 O11
• Title of publication: Efficient syntheses of macrocycles ranging from 22‒28 atoms through spontaneous dimerization to yield bis-hydrazones
• Authors of publication: Sharma, Vishal R.; Mehmood, Arshad; Janesko, Benjamin G.; Simanek, Eric E.
• Journal of publication: RSC Advances
• Year of publication: 2020
• Journal volume: 10
• Journal issue: 6
• Pages of publication: 3217 - 3220
• a: 10.022 ± 0.0003 Å
• b: 13.0296 ± 0.0004 Å
• c: 18.2777 ± 0.0005 Å
• α: 102.894 ± 0.001°
• β: 95.754 ± 0.001°
• γ: 103.889 ± 0.001°
• Cell volume: 2228.51 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0945
• Residual factor for significantly intense reflections: 0.0793
• Weighted residual factors for significantly intense reflections: 0.2154
• Weighted residual factors for all reflections included in the refinement: 0.2318
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No