Information card for entry 7239803

Structure parameters

• Formula: C25 H52 N2 Si3
• Calculated formula: C25 H52 N2 Si3
• Title of publication: DMAP-stabilized bis(silyl)silylenes as versatile synthons for organosilicon compounds
• Authors of publication: Holzner, Richard; Reiter, Dominik; Frisch, Philipp; Inoue, Shigeyoshi
• Journal of publication: RSC Advances
• Year of publication: 2020
• Journal volume: 10
• Journal issue: 6
• Pages of publication: 3402 - 3406
• a: 11.977 ± 0.0013 Å
• b: 16.9418 ± 0.0017 Å
• c: 28.631 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5809.6 ± 1.1 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0334
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0771
• Weighted residual factors for all reflections included in the refinement: 0.0802
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No