Information card for entry 7240112

Structure parameters

• Formula: C14 H22 Cl8 N4 Zn2
• Calculated formula: C14 H22 Cl8 N4 Zn2
• Title of publication: Effect of stepwise protonation of an N-containing ligand on the formation of metal-organic salts and coordination complexes in the solid state
• Authors of publication: Lu, Hai Dong; Li, Hai Tao; Xin, Lianxin; Guo, Fang
• Journal of publication: CrystEngComm
• Year of publication: 2020
• a: 10.2666 ± 0.0006 Å
• b: 9.5232 ± 0.0006 Å
• c: 13.0868 ± 0.0008 Å
• α: 90°
• β: 106.857 ± 0.002°
• γ: 90°
• Cell volume: 1224.53 ± 0.13 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0287
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.0662
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71076 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No