Information card for entry 7240229

Structure parameters

• Formula: C28 H35 N P2
• Calculated formula: C28 H20 N P2
• Title of publication: Synthesis of 1,2,4-azadiphosphole derivatives based on vanadium-catalyzed [2+2+1] cycloaddition reactions of azobenzenes with phosphaalkynes
• Authors of publication: Liang, Wenbin; Nakajima, Kazunari; Nishibayashi, Yoshiaki
• Journal of publication: RSC Advances
• Year of publication: 2020
• Journal volume: 10
• Journal issue: 22
• Pages of publication: 12730 - 12733
• a: 14.242 ± 0.0009 Å
• b: 10.3185 ± 0.0007 Å
• c: 16.3776 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2406.8 ± 0.3 ų
• Cell temperature: 178 K
• Ambient diffraction temperature: 178 K
• Number of distinct elements: 4
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.1625
• Residual factor for significantly intense reflections: 0.1398
• Weighted residual factors for significantly intense reflections: 0.2387
• Weighted residual factors for all reflections included in the refinement: 0.2519
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No