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Information card for entry 7240267
Preview
Coordinates | 7240267.cif |
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Original paper (by DOI) | HTML |
Formula | C26 H25 Cl N2 O4 |
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Calculated formula | C26 H25 Cl N2 O4 |
Title of publication | Synthesis of 1,3-diaryl-spiro[azetidine-2,3′-indoline]-2′,4-diones via the Staudinger reaction: cis- or trans-diastereoselectivity with different addition modes |
Authors of publication | Filatov, Vadim; Kukushkin, Maksim; Kuznetsova, Juliana; Skvortsov, Dmitry; Tafeenko, Viktor; Zyk, Nikolay; Majouga, Alexander; Beloglazkina, Elena |
Journal of publication | RSC Advances |
Year of publication | 2020 |
Journal volume | 10 |
Journal issue | 24 |
Pages of publication | 14122 - 14133 |
a | 9.8999 ± 0.0003 Å |
b | 15.9931 ± 0.0004 Å |
c | 15.6852 ± 0.0005 Å |
α | 90° |
β | 104.928 ± 0.003° |
γ | 90° |
Cell volume | 2399.62 ± 0.13 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0711 |
Residual factor for significantly intense reflections | 0.0439 |
Weighted residual factors for significantly intense reflections | 0.1165 |
Weighted residual factors for all reflections included in the refinement | 0.1292 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.929 |
Diffraction radiation wavelength | 1.54186 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7240267.html
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