Information card for entry 7240491

Structure parameters

• Formula: C7 H12 K3.5 O20 Sc
• Calculated formula: C7 H12 K3.5 O20 Sc
• Title of publication: Solvent-free ageing reactions of rare earth element oxides: from geomimetic synthesis of new metal‒organic materials towards a simple, environmentally friendly separation of scandium
• Authors of publication: Huskić, Igor; Arhangelskis, Mihails; Friščić, Tomislav
• Journal of publication: Green Chemistry
• Year of publication: 2020
• Journal volume: 22
• Journal issue: 13
• Pages of publication: 4364 - 4375
• a: 15.8839 ± 0.0014 Å
• b: 11.4558 ± 0.001 Å
• c: 22.7314 ± 0.0019 Å
• α: 90°
• β: 92.19 ± 0.004°
• γ: 90°
• Cell volume: 4133.2 ± 0.6 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1263
• Weighted residual factors for all reflections included in the refinement: 0.1425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No