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Information card for entry 7240640
Preview
Coordinates | 7240640.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C7 H22 N O4 P |
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Calculated formula | C7 H22 N O4 P |
SMILES | P(=O)([O-])C[NH+](C(C)C)C(C)C.O.O |
Title of publication | Selective and clean synthesis of aminoalkyl-H-phosphinic acids from hypophosphorous acid by phospha-Mannich reaction |
Authors of publication | Urbanovský, Peter; Kotek, Jan; Císařová, Ivana; Hermann, Petr |
Journal of publication | RSC Advances |
Year of publication | 2020 |
Journal volume | 10 |
Journal issue | 36 |
Pages of publication | 21329 - 21349 |
a | 13.364 ± 0.0006 Å |
b | 8.5851 ± 0.0004 Å |
c | 20.1404 ± 0.0011 Å |
α | 90° |
β | 91.384 ± 0.002° |
γ | 90° |
Cell volume | 2310.1 ± 0.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0329 |
Residual factor for significantly intense reflections | 0.0288 |
Weighted residual factors for significantly intense reflections | 0.0746 |
Weighted residual factors for all reflections included in the refinement | 0.0767 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7240640.html
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Users of the data should acknowledge the original authors of the
structural data.