Proline derived guanidine catalysts forge extensive H-bonded architectures: a solution and solid state study
Authors of publication
Al-Taie, Zahraa S.; Anetts, Simon R.; Christensen, Jeppe; Coles, Simon J.; Horton, Peter N.; Evans, Daniel M.; Jones, Leigh F.; de Kleijne, Frank F. J.; Ledbetter, Shaun M.; Mehdar, Yassin T. H.; Murphy, Patrick J.; Wilson, Jack A.
Journal of publication
RSC Advances
Year of publication
2020
Journal volume
10
Journal issue
38
Pages of publication
22397 - 22416
a
12.4402 ± 0.0004 Å
b
12.933 ± 0.0004 Å
c
19.1393 ± 0.0006 Å
α
90°
β
99.889 ± 0.003°
γ
90°
Cell volume
3033.55 ± 0.17 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
I 1 2/a 1
Hall space group symbol
-I 2ya
Residual factor for all reflections
0.1479
Residual factor for significantly intense reflections
0.1348
Weighted residual factors for significantly intense reflections
0.2896
Weighted residual factors for all reflections included in the refinement
0.2952
Goodness-of-fit parameter for all reflections included in the refinement
