Information card for entry 7240910

Structure parameters

• Formula: C8 H9 Cl3 N2 Pb
• Calculated formula: C8 H9 Cl3 N2 Pb
• Title of publication: Synthetic strategy towards halometallates with imidazo[1,5-a]pyridinium-based counterions
• Authors of publication: Vassilyeva, Olga Yu.; Buvaylo, Elena A.; Linnik, Rostyslav P.; Nesterov, Dmytro S.; Trachevsky, Vladimir V.; Skelton, Brian W.
• Journal of publication: CrystEngComm
• Year of publication: 2020
• a: 43.5467 ± 0.0012 Å
• b: 24.859 ± 0.0007 Å
• c: 4.3222 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4678.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.026
• Residual factor for significantly intense reflections: 0.0204
• Weighted residual factors for significantly intense reflections: 0.0304
• Weighted residual factors for all reflections included in the refinement: 0.0318
• Goodness-of-fit parameter for all reflections included in the refinement: 0.875
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No