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Information card for entry 7241168
Preview
Coordinates | 7241168.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H19 Br N O P S |
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Calculated formula | C27 H19 Br N O P S |
Title of publication | Copper(ii)-catalyzed tandem cyclization for the synthesis of benzo[d][1,3]thiazin-2-yl phosphonates involving C‒P and C‒S bond formation |
Authors of publication | Liu, Yang; Yao, Shijie; Wang, Chaoli; Zhang, Yahui; Hao, Wenyan |
Journal of publication | RSC Advances |
Year of publication | 2020 |
Journal volume | 10 |
Journal issue | 53 |
Pages of publication | 32211 - 32215 |
a | 8.7427 ± 0.0006 Å |
b | 11.4201 ± 0.0007 Å |
c | 12.4832 ± 0.0009 Å |
α | 82.935 ± 0.006° |
β | 73.455 ± 0.007° |
γ | 75.613 ± 0.006° |
Cell volume | 1155.45 ± 0.14 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0705 |
Residual factor for significantly intense reflections | 0.0465 |
Weighted residual factors for significantly intense reflections | 0.1157 |
Weighted residual factors for all reflections included in the refinement | 0.1287 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7241168.html
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Users of the data should acknowledge the original authors of the
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