Information card for entry 7241966

Structure parameters

• Formula: C32 H16 N16 O7 Rb4 W2
• Calculated formula: C32 H16 N16 O7 Rb4 W2
• Title of publication: X-ray crystal structures of K+ and Rb+ salts of [W(CN)6(bpy)]2− ion. The unusual cation‒anion interactions and structure changes going from Li+ to Cs+ salts
• Authors of publication: Hodorowicz, Maciej; Jurowska, Anna; Szklarzewicz, Janusz
• Journal of publication: CrystEngComm
• Year of publication: 2021
• Journal volume: 23
• Journal issue: 5
• Pages of publication: 1207 - 1217
• a: 26.6594 ± 0.0003 Å
• b: 9.2333 ± 0.0001 Å
• c: 17.6019 ± 0.0002 Å
• α: 90°
• β: 93.22 ± 0.001°
• γ: 90°
• Cell volume: 4325.94 ± 0.08 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.0907
• Weighted residual factors for all reflections included in the refinement: 0.0967
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No