Crystallography Open Database

Information card for entry 7242622

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Coordinates	7242622.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H23 N O
Calculated formula	C25 H23 N O
Title of publication	Bimetallic aluminum complexes bearing novel spiro-phenanthrene-monoketone/OH derivatives: synthesis, characterization and the ring-opening polymerization of ε-caprolactone
Authors of publication	Yue, Erlin; Cao, Furong; Zhang, Jun; Zhang, Wenjuan; Jiang, Youshu; Liang, Tongling; Sun, Wen-Hua
Journal of publication	RSC Advances
Year of publication	2021
Journal volume	11
Journal issue	22
Pages of publication	13274 - 13281
a	9.2698 ± 0.0019 Å
b	18.914 ± 0.004 Å
c	21.689 ± 0.004 Å
α	90°
β	93.87 ± 0.03°
γ	90°
Cell volume	3794 ± 1.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1291
Residual factor for significantly intense reflections	0.1071
Weighted residual factors for significantly intense reflections	0.2185
Weighted residual factors for all reflections included in the refinement	0.2384
Goodness-of-fit parameter for all reflections included in the refinement	1.005
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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