Information card for entry 7242634

Structure parameters

• Formula: C32 H24 Co2 N8 O48 Si W12
• Calculated formula: C32 H24 Co2 N8 O48 Si W12
• Title of publication: Assembly, structures and properties of polyoxometalate-based supramolecular complexes involving in situ transformation of single-branch N-donor cyano ligands
• Authors of publication: Wang, Xiang; Li, Yunhui; Zhang, Tong; Ma, Sijia; Wang, Xiuli
• Journal of publication: CrystEngComm
• Year of publication: 2021
• Journal volume: 23
• Journal issue: 19
• Pages of publication: 3477 - 3487
• a: 11.2593 ± 0.0009 Å
• b: 12.2095 ± 0.001 Å
• c: 12.6834 ± 0.0011 Å
• α: 77.379 ± 0.002°
• β: 70.498 ± 0.002°
• γ: 88.223 ± 0.002°
• Cell volume: 1602.2 ± 0.2 ų
• Cell temperature: 273.15 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1595
• Weighted residual factors for all reflections included in the refinement: 0.165
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No