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Information card for entry 7242691
Preview
Coordinates | 7242691.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H33 N O6 |
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Calculated formula | C32 H33 N O6 |
Title of publication | Tin(iv) chloride mediated (3 + 2) annulation of trans-2-aroyl-3-styrylcyclopropane-1,1-dicarboxylates with nitriles: diastereoselective access to 5-vinyl-1-pyrroline derivatives |
Authors of publication | Thangamani, Murugesan; Thangamalar, Subaramaniam; Srinivasan, Kannupal |
Journal of publication | RSC Advances |
Year of publication | 2021 |
Journal volume | 11 |
Journal issue | 25 |
Pages of publication | 14980 - 14985 |
a | 10.0422 ± 0.0006 Å |
b | 22.1419 ± 0.0014 Å |
c | 26.2315 ± 0.0015 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5832.7 ± 0.6 Å3 |
Cell temperature | 298.08 K |
Ambient diffraction temperature | 298.08 K |
Number of distinct elements | 4 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.1641 |
Residual factor for significantly intense reflections | 0.0723 |
Weighted residual factors for significantly intense reflections | 0.1645 |
Weighted residual factors for all reflections included in the refinement | 0.2208 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7242691.html
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Users of the data should acknowledge the original authors of the
structural data.