Information card for entry 7242946
| Formula |
C22 H18 F3 N3 |
| Calculated formula |
C22 H18 F3 N3 |
| Title of publication |
Aminations and arylations by direct C‒O activation for the design of 7,8-dihydro-6H-5,8-ethanopyrido[3,2-d]pyrimidines |
| Authors of publication |
Laurent, Mazarine; Bostyn, Stéphane; Marchivie, Mathieu; Robin, Yves; Routier, Sylvain; Buron, Frédéric |
| Journal of publication |
RSC Advances |
| Year of publication |
2021 |
| Journal volume |
11 |
| Journal issue |
32 |
| Pages of publication |
19363 - 19377 |
| a |
15.3849 ± 0.0012 Å |
| b |
5.8934 ± 0.0004 Å |
| c |
22.187 ± 0.002 Å |
| α |
90° |
| β |
110.051 ± 0.004° |
| γ |
90° |
| Cell volume |
1889.7 ± 0.3 Å3 |
| Cell temperature |
299.59 K |
| Ambient diffraction temperature |
299.59 K |
| Number of distinct elements |
4 |
| Space group number |
4 |
| Hermann-Mauguin space group symbol |
P 1 21 1 |
| Hall space group symbol |
P 2yb |
| Residual factor for all reflections |
0.082 |
| Residual factor for significantly intense reflections |
0.0543 |
| Weighted residual factors for significantly intense reflections |
0.1351 |
| Weighted residual factors for all reflections included in the refinement |
0.1503 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.043 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7242946.html
