Information card for entry 7242970
| Formula |
C32 H23 N O6 S |
| Calculated formula |
C32 H23 N O6 S |
| Title of publication |
Construction of cyclopentane-fused coumarins via DBU-catalyzed [3+2] cycloaddition of 3-homoacyl coumarins with cyclic 1-azadienes |
| Authors of publication |
Lin, Huawei; Yang, Huimin; Gong, Qi; Luo, Shan; Gu, Jing; Cao, Xiaoqun; Mao, Biming; Ge, Yanqing; Yuan, Chunhao |
| Journal of publication |
RSC Advances |
| Year of publication |
2021 |
| Journal volume |
11 |
| Journal issue |
33 |
| Pages of publication |
20118 - 20122 |
| a |
10.5537 ± 0.001 Å |
| b |
11.0474 ± 0.0011 Å |
| c |
13.2402 ± 0.0013 Å |
| α |
114.381 ± 0.003° |
| β |
99 ± 0.003° |
| γ |
101.915 ± 0.003° |
| Cell volume |
1324.2 ± 0.2 Å3 |
| Cell temperature |
193 ± 2 K |
| Ambient diffraction temperature |
193 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0793 |
| Residual factor for significantly intense reflections |
0.0758 |
| Weighted residual factors for significantly intense reflections |
0.2104 |
| Weighted residual factors for all reflections included in the refinement |
0.2158 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.039 |
| Diffraction radiation wavelength |
1.34139 Å |
| Diffraction radiation type |
GaKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7242970.html
