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Information card for entry 7243402
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Coordinates | 7243402.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C47 H41 Cl3 N4 O4 |
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Calculated formula | C47 H41 Cl3 N4 O4 |
Title of publication | TMSOTf-catalyzed synthesis of trisubstituted imidazoles using hexamethyldisilazane as a nitrogen source under neat and microwave irradiation conditions |
Authors of publication | Asressu, Kesatebrhan Haile; Chan, Chieh-Kai; Wang, Cheng-Chung |
Journal of publication | RSC Advances |
Year of publication | 2021 |
Journal volume | 11 |
Journal issue | 45 |
Pages of publication | 28061 - 28071 |
a | 10.237 ± 0.0004 Å |
b | 18.3683 ± 0.0006 Å |
c | 22.354 ± 0.0008 Å |
α | 90° |
β | 95.807 ± 0.001° |
γ | 90° |
Cell volume | 4181.8 ± 0.3 Å3 |
Cell temperature | 100 ± 0.2 K |
Ambient diffraction temperature | 100 ± 0.2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0857 |
Residual factor for significantly intense reflections | 0.0627 |
Weighted residual factors for significantly intense reflections | 0.1759 |
Weighted residual factors for all reflections included in the refinement | 0.1928 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.054 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7243402.html
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Users of the data should acknowledge the original authors of the
structural data.