Information card for entry 7243624

Structure parameters

• Formula: C57 H120 N15 O6 V3
• Calculated formula: C57 H120 N15 O6 V3
• Title of publication: Synthesis of cyanooxovanadate and cyanosilylation of ketones
• Authors of publication: Kikukawa, Yuji; Kawabata, Hiroko; Hayashi, Yoshihito
• Journal of publication: RSC Advances
• Year of publication: 2021
• Journal volume: 11
• Journal issue: 50
• Pages of publication: 31688 - 31692
• a: 8.24 ± 0.0002 Å
• b: 34.3199 ± 0.0008 Å
• c: 12.7556 ± 0.0003 Å
• α: 90°
• β: 93.197 ± 0.001°
• γ: 90°
• Cell volume: 3601.62 ± 0.15 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0835
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for significantly intense reflections: 0.1832
• Weighted residual factors for all reflections included in the refinement: 0.194
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No