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Information card for entry 7244110
Preview
Coordinates | 7244110.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H28 N2 O8 |
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Calculated formula | C31 H28 N2 O8 |
Title of publication | Cycloaddition of Huisgen 1,4-dipoles: synthesis and rapid epimerization of functionalized spiropyrido[2,1-<i>b</i>][1,3]oxazine-pyrroles and related products. |
Authors of publication | Galeev, Andrew R.; Moroz, Anna A.; Dmitriev, Maksim V.; Maslivets, Andrey N. |
Journal of publication | RSC advances |
Year of publication | 2021 |
Journal volume | 12 |
Journal issue | 1 |
Pages of publication | 578 - 587 |
a | 11.1868 ± 0.0016 Å |
b | 11.4255 ± 0.0018 Å |
c | 12.2739 ± 0.0016 Å |
α | 95.263 ± 0.012° |
β | 107.966 ± 0.012° |
γ | 103.507 ± 0.013° |
Cell volume | 1428.1 ± 0.4 Å3 |
Cell temperature | 295.15 K |
Ambient diffraction temperature | 295.15 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.087 |
Residual factor for significantly intense reflections | 0.0592 |
Weighted residual factors for significantly intense reflections | 0.1542 |
Weighted residual factors for all reflections included in the refinement | 0.1804 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7244110.html
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Users of the data should acknowledge the original authors of the
structural data.