Information card for entry 7244608

Structure parameters

• Formula: C24 H17 N O2
• Calculated formula: C24 H17 N O2
• Title of publication: TMSOTf-mediated Kröhnke pyridine synthesis using HMDS as the nitrogen source under microwave irradiation
• Authors of publication: Chan, Chieh-Kai; Chung, Yi-Hsiu; Wang, Cheng-Chung
• Journal of publication: RSC Advances
• Year of publication: 2022
• Journal volume: 12
• Journal issue: 13
• Pages of publication: 8263 - 8273
• a: 6.4058 ± 0.0002 Å
• b: 12.1092 ± 0.0003 Å
• c: 21.6453 ± 0.0007 Å
• α: 90°
• β: 92.249 ± 0.001°
• γ: 90°
• Cell volume: 1677.71 ± 0.09 ų
• Cell temperature: 100 ± 0.2 K
• Ambient diffraction temperature: 100 ± 0.2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0412
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.0912
• Weighted residual factors for all reflections included in the refinement: 0.0956
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No