Information card for entry 7244671

Structure parameters

• Formula: C19 H22 O6
• Calculated formula: C19 H22 O6
• Title of publication: Highly efficient construction of an oxa-[3.2.1]octane-embedded 5–7–6 tricyclic carbon skeleton and ring-opening of the bridged ring via C–O bond cleavage
• Authors of publication: Cui, Yi; Lv, Jiayuan; Song, Tianhang; Ren, Jun; Wang, Zhongwen
• Journal of publication: RSC Advances
• Year of publication: 2022
• Journal volume: 12
• Journal issue: 16
• Pages of publication: 9519 - 9523
• a: 27.2898 ± 0.001 Å
• b: 7.681 ± 0.0003 Å
• c: 16.4376 ± 0.0006 Å
• α: 90°
• β: 98.219 ± 0.004°
• γ: 90°
• Cell volume: 3410.1 ± 0.2 ų
• Cell temperature: 113.15 K
• Ambient diffraction temperature: 113.15 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.068
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1145
• Weighted residual factors for all reflections included in the refinement: 0.1273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No