Bulky countercation effects on the crystal packing of anionic dithiooxalato-containing Ni(II), Pd(II) and Pt(II) complexes: spectroscopic-redox correlations
Authors of publication
Julve, Miguel; El Alouani Dahmouni, Nadia; Switlicka, Anna; Machura, B.; Moliner, Fernando Nicolás; Rabelo, Renato; Ruiz-Garcia, Rafael; Stiriba, Salah-Eddine; Cano, Joan
Journal of publication
CrystEngComm
Year of publication
2022
a
8.8748 ± 0.0003 Å
b
16.807 ± 0.0005 Å
c
15.6789 ± 0.0005 Å
α
90°
β
96.144 ± 0.001°
γ
90°
Cell volume
2325.21 ± 0.13 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120.01 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0394
Residual factor for significantly intense reflections
0.0261
Weighted residual factors for significantly intense reflections
0.0435
Weighted residual factors for all reflections included in the refinement
0.0466
Goodness-of-fit parameter for all reflections included in the refinement
