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Information card for entry 7245401
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Coordinates | 7245401.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H63 Fe3 Mn O6 |
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Calculated formula | C54 H63 Fe3 Mn O6 |
Title of publication | Stereoselective synthesis of the isoxazolidine ring via manganese(iii)-catalysed aminoperoxidation of unactivated alkenes using molecular oxygen in air under ambient conditions |
Authors of publication | Yamamoto, Daisuke; Hirano, Issei; Narushima, Yuki; Soga, Masayuki; Ansai, Hiromasa; Makino, Kazuishi |
Journal of publication | Green Chemistry |
Year of publication | 2022 |
Journal volume | 24 |
Journal issue | 18 |
Pages of publication | 7162 - 7170 |
a | 11.5777 ± 0.0002 Å |
b | 23.2895 ± 0.0004 Å |
c | 17.4903 ± 0.0003 Å |
α | 90° |
β | 92.923 ± 0.007° |
γ | 90° |
Cell volume | 4709.93 ± 0.14 Å3 |
Cell temperature | 93 K |
Ambient diffraction temperature | 93 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1145 |
Residual factor for significantly intense reflections | 0.0785 |
Weighted residual factors for significantly intense reflections | 0.1957 |
Weighted residual factors for all reflections included in the refinement | 0.2166 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.081 |
Diffraction radiation wavelength | 1.54187 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7245401.html
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structural data.