Information card for entry 7245574

Structure parameters

• Formula: C24 H23 Cl3 N2 O3
• Calculated formula: C24 H23 Cl3 N2 O3
• Title of publication: Synthesis of dihydroindazolo[2,3-f]phenanthridin-5(6H)-ones via Rh(iii)-catalyzed C–H activation of 2-aryl indazoles and annulation with iodonium ylides
• Authors of publication: Liang, Jiazhi; Huang, Jian; Yang, Qin; Fu, Yang; Ding, Qiuping; Peng, Yiyuan
• Journal of publication: Green Chemistry
• Year of publication: 2022
• Journal volume: 24
• Journal issue: 21
• Pages of publication: 8441 - 8446
• a: 5.819 ± 0.0002 Å
• b: 9.8242 ± 0.0004 Å
• c: 20.3104 ± 0.001 Å
• α: 92.796 ± 0.004°
• β: 92.658 ± 0.003°
• γ: 95.189 ± 0.003°
• Cell volume: 1153.44 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0544
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1082
• Weighted residual factors for all reflections included in the refinement: 0.1154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No