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Information card for entry 7245608
Preview
Coordinates | 7245608.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H27 F7 N4 O4 |
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Calculated formula | C28 H27 F7 N4 O4 |
Title of publication | Four-component defluorinative reaction of allylic fluorides, amidines, and Cs2CO3 under transition-metal-free conditions |
Authors of publication | Chen, Yu-Lan; Sun, Li-Wen; Chen, Jia-Wei; Zhu, Ming-Quan; Ma, Mengtao; Shen, Zhi-Liang; Chu, Xue-Qiang |
Journal of publication | Green Chemistry |
Year of publication | 2022 |
Journal volume | 24 |
Journal issue | 18 |
Pages of publication | 6816 - 6822 |
a | 9.8007 ± 0.0008 Å |
b | 19.457 ± 0.0018 Å |
c | 15.5025 ± 0.0012 Å |
α | 90° |
β | 99.565 ± 0.007° |
γ | 90° |
Cell volume | 2915.1 ± 0.4 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1359 |
Residual factor for significantly intense reflections | 0.0926 |
Weighted residual factors for significantly intense reflections | 0.2199 |
Weighted residual factors for all reflections included in the refinement | 0.2673 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.005 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7245608.html
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Users of the data should acknowledge the original authors of the
structural data.