Information card for entry 7245747

Structure parameters

• Formula: C15 H25 N O2
• Calculated formula: C15 H25 N O2
• Title of publication: Annulated carbamates are precursors for the ring contraction of the adamantane framework
• Authors of publication: Hrdina, Radim; Holovko-Kamoshenkova, Oksana M.; Císařová, Ivana; Koucký, Filip; Machalický, Oldřich
• Journal of publication: RSC Advances
• Year of publication: 2022
• Journal volume: 12
• Journal issue: 48
• Pages of publication: 31056 - 31060
• a: 12.2381 ± 0.0005 Å
• b: 11.7529 ± 0.0006 Å
• c: 10.0683 ± 0.0004 Å
• α: 90°
• β: 105.123 ± 0.003°
• γ: 90°
• Cell volume: 1398 ± 0.11 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0629
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.0994
• Weighted residual factors for all reflections included in the refinement: 0.109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No