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Information card for entry 7246764
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Coordinates | 7246764.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H38 Cl O3 P |
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Calculated formula | C31 H38 Cl O3 P |
Title of publication | Tandem addition of nucleophilic and electrophilic reagents to vinyl phosphinates: the stereoselective formation of organophosphorus compounds with congested tertiary carbons |
Authors of publication | Lin, Zhu; Zhai, De-Hua; Sun, Yong-Ming; Zheng, Hong-Xing; Li, Qiang; Wang, Yan-Lan; Wen, Jing-Hong; Zhao, Chang-Qiu |
Journal of publication | RSC Advances |
Year of publication | 2023 |
Journal volume | 13 |
Journal issue | 21 |
Pages of publication | 14060 - 14064 |
a | 6.5468 ± 0.0007 Å |
b | 16.2047 ± 0.0016 Å |
c | 27.749 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2943.9 ± 0.5 Å3 |
Cell temperature | 298.15 K |
Ambient diffraction temperature | 298.15 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1602 |
Residual factor for significantly intense reflections | 0.074 |
Weighted residual factors for significantly intense reflections | 0.1692 |
Weighted residual factors for all reflections included in the refinement | 0.2052 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.874 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7246764.html
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Users of the data should acknowledge the original authors of the
structural data.