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Information card for entry 7246990
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Coordinates | 7246990.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H22 N O5 |
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Calculated formula | C24 H22 N O5 |
Title of publication | POCl<sub>3</sub> mediated one-pot deoxygenative aromatization and electrophilic chlorination of dihydroxy-2-methyl-4-oxo-indeno[1,2-<i>b</i>]pyrroles. |
Authors of publication | Nasuhipur, Forough; Ghasemi, Zarrin; Poupon, Morgane; Dušek, Michal |
Journal of publication | RSC advances |
Year of publication | 2023 |
Journal volume | 13 |
Journal issue | 26 |
Pages of publication | 17812 - 17816 |
a | 8.8388 ± 0.0003 Å |
b | 21.2913 ± 0.0005 Å |
c | 10.8389 ± 0.0004 Å |
α | 90° |
β | 91.297 ± 0.003° |
γ | 90° |
Cell volume | 2039.25 ± 0.11 Å3 |
Cell temperature | 95 ± 0.4 K |
Ambient diffraction temperature | 95 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0869 |
Residual factor for significantly intense reflections | 0.0757 |
Weighted residual factors for significantly intense reflections | 0.2459 |
Weighted residual factors for all reflections included in the refinement | 0.2472 |
Goodness-of-fit parameter for significantly intense reflections | 4.3015 |
Goodness-of-fit parameter for all reflections included in the refinement | 3.776 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7246990.html
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Users of the data should acknowledge the original authors of the
structural data.