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Information card for entry 7247299
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Coordinates | 7247299.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H27 N O |
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Calculated formula | C36 H27 N O |
Title of publication | Green and effective synthesis of multisubstituted α-pyrones via K2CO3 catalyzed formal insertion of ketenimines into C(CO)–C bonds of 1,3-diketones |
Authors of publication | Luo, Jian; Zhong, Ai-Qing; Qiu, Jia-Hao; Liu, Xiong-Wei; Tian, You-Ping; Zhang, Bao-Hua; Chen, Guo-Shu; Shu, Wei; Liu, Yun-Lin |
Journal of publication | Green Chemistry |
Year of publication | 2023 |
Journal volume | 25 |
Journal issue | 20 |
Pages of publication | 8057 - 8067 |
a | 10.3653 ± 0.0009 Å |
b | 11.5399 ± 0.0008 Å |
c | 12.1483 ± 0.0009 Å |
α | 86.936 ± 0.006° |
β | 75.711 ± 0.007° |
γ | 69.063 ± 0.007° |
Cell volume | 1314.21 ± 0.19 Å3 |
Cell temperature | 170 ± 0.1 K |
Ambient diffraction temperature | 170 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0652 |
Residual factor for significantly intense reflections | 0.0485 |
Weighted residual factors for significantly intense reflections | 0.1269 |
Weighted residual factors for all reflections included in the refinement | 0.1374 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.164 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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