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Information card for entry 7247301
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Coordinates | 7247301.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H27 N O5 |
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Calculated formula | C29 H27 N O5 |
Title of publication | Green and effective synthesis of multisubstituted α-pyrones via K2CO3 catalyzed formal insertion of ketenimines into C(CO)–C bonds of 1,3-diketones |
Authors of publication | Luo, Jian; Zhong, Ai-Qing; Qiu, Jia-Hao; Liu, Xiong-Wei; Tian, You-Ping; Zhang, Bao-Hua; Chen, Guo-Shu; Shu, Wei; Liu, Yun-Lin |
Journal of publication | Green Chemistry |
Year of publication | 2023 |
Journal volume | 25 |
Journal issue | 20 |
Pages of publication | 8057 - 8067 |
a | 11.0361 ± 0.0005 Å |
b | 14.2348 ± 0.0005 Å |
c | 16.7656 ± 0.0006 Å |
α | 79.529 ± 0.003° |
β | 88.302 ± 0.003° |
γ | 75.05 ± 0.004° |
Cell volume | 2501.88 ± 0.18 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0963 |
Residual factor for significantly intense reflections | 0.0603 |
Weighted residual factors for significantly intense reflections | 0.1368 |
Weighted residual factors for all reflections included in the refinement | 0.1608 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7247301.html
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Users of the data should acknowledge the original authors of the
structural data.