Information card for entry 7248023

Structure parameters

• Formula: C74 H84 N14 Ni3 O31
• Calculated formula: C66 H60 N12 Ni3 O24
• Title of publication: Construction and catalytic effects of solvent- and metal(ii)-dependent products: the process of transformation of 0D structures into 3D structures
• Authors of publication: Kim, Gyeongmin; Han, Jihun; Kim, Dongwon; Jung, Ok-Sang
• Journal of publication: CrystEngComm
• Year of publication: 2024
• Journal volume: 26
• Journal issue: 7
• Pages of publication: 918 - 925
• a: 14.608 ± 0.002 Å
• b: 14.608 ± 0.002 Å
• c: 24.244 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4480.4 ± 1.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 147
• Hermann-Mauguin space group symbol: P -3
• Hall space group symbol: -P 3
• Residual factor for all reflections: 0.1829
• Residual factor for significantly intense reflections: 0.1458
• Weighted residual factors for significantly intense reflections: 0.3727
• Weighted residual factors for all reflections included in the refinement: 0.4034
• Goodness-of-fit parameter for all reflections included in the refinement: 1.389
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No