Information card for entry 7248592

Structure parameters

• Formula: C24 H24 N2 O6
• Calculated formula: C24 H24 N2 O6
• Title of publication: Sequential Glaser reaction-diastereoselective cyclocarboxylation of propargylamines with CO2: A green catalytic access to bis-oxazolidinonedienes and their topochemical polymerization
• Authors of publication: Mele, Francesco; Constantin, Ana Maria; Sacchelli, Filippo; Schiroli, Debora; Mazzeo, Paolo Pio; Maestri, Giovanni; Motti, Elena; Maggi, Raimondo; Mancuso, Raffaella; Gabriele, Bartolo; Pancrazzi, francesco; Della Ca', Nicola
• Journal of publication: Green Chemistry
• Year of publication: 2024
• a: 40.9802 ± 0.0007 Å
• b: 5.9856 ± 0.0001 Å
• c: 8.7293 ± 0.0002 Å
• α: 90°
• β: 97.256 ± 0.001°
• γ: 90°
• Cell volume: 2124.07 ± 0.07 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.0901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No