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Information card for entry 7248732
Preview
Coordinates | 7248732.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H11 N O4 S |
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Calculated formula | C15 H11 N O4 S |
Title of publication | Base mediated aza-[2 + 1] annulation and regioselective aziridine ring-opening cascade: mild synthesis of functionalized β-amino ketones from cyclic N-sulfonyl aldimines and α-carbonyl sulfonium salts |
Authors of publication | Lei, Xiaoqiang; Sun, Yanyan; Guo, Qinglan; Shi, Jiangong |
Journal of publication | RSC Advances |
Year of publication | 2024 |
Journal volume | 14 |
Journal issue | 24 |
Pages of publication | 17178 - 17183 |
a | 17.0912 ± 0.0003 Å |
b | 5.88627 ± 0.0001 Å |
c | 13.7901 ± 0.0003 Å |
α | 90° |
β | 109.188 ± 0.002° |
γ | 90° |
Cell volume | 1310.26 ± 0.05 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0416 |
Residual factor for significantly intense reflections | 0.0396 |
Weighted residual factors for significantly intense reflections | 0.1085 |
Weighted residual factors for all reflections included in the refinement | 0.1101 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7248732.html
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Users of the data should acknowledge the original authors of the
structural data.