Crystallography Open Database

Information card for entry 7249109

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Coordinates	7249109.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H15 N
Calculated formula	C20 H15 N
Title of publication	A concise protocol for the synthesis of 2-alkenylindoles through [4 + 1] annulation of aminobenzyl phosphonium salts with acrylaldehydes
Authors of publication	Yang, Jia-Cheng; Liao, Mao-Lin; Li, Ping-Gui; Zou, Liang-Hua
Journal of publication	Green Chemistry
Year of publication	2024
Journal volume	26
Journal issue	17
Pages of publication	9295 - 9299
a	16.0588 ± 0.0007 Å
b	10.0682 ± 0.0004 Å
c	18.9261 ± 0.0008 Å
α	90°
β	103.229 ± 0.002°
γ	90°
Cell volume	2978.8 ± 0.2 Å³
Cell temperature	302 ± 2 K
Ambient diffraction temperature	302.15 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0662
Residual factor for significantly intense reflections	0.0457
Weighted residual factors for significantly intense reflections	0.1201
Weighted residual factors for all reflections included in the refinement	0.1353
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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