Information card for entry 7249242

Structure parameters

• Formula: C24 H26 I2 N4 Pd
• Calculated formula: C24 H26 I2 N4 Pd
• Title of publication: Palladium(ii) complexes bearing mesoionic carbene ligands: catalytic application in domino Sonogashira coupling/cyclization reactions for one-pot synthesis of benzofuran and indole derivatives.
• Authors of publication: Joshi, Om Prakash; Thirumoorthi, Ramalingam; Pardasani, Ram T.; Ray, Sriparna; Dash, Chandrakanta
• Journal of publication: RSC advances
• Year of publication: 2024
• Journal volume: 14
• Journal issue: 37
• Pages of publication: 27141 - 27152
• a: 9.578 ± 0.0003 Å
• b: 16.2412 ± 0.0006 Å
• c: 33.3733 ± 0.0012 Å
• α: 90°
• β: 96.353 ± 0.001°
• γ: 90°
• Cell volume: 5159.6 ± 0.3 ų
• Cell temperature: 145 ± 2 K
• Ambient diffraction temperature: 145 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.0883
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.206
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No