Information card for entry 7249371

Structure parameters

• Formula: C23 H27 Cl2 N5 Ni O10
• Calculated formula: C23 H27 Cl2 N5 Ni O10
• Title of publication: Selective synthesis of cyclic alcohols from cycloalkanes using nickel(ii) complexes of tetradentate amidate ligands
• Authors of publication: Rajeev, Anjana; Muthuramalingam, Sethuraman; Sankaralingam, Muniyandi
• Journal of publication: RSC Advances
• Year of publication: 2024
• Journal volume: 14
• Journal issue: 41
• Pages of publication: 30440 - 30451
• a: 17.786 ± 0.003 Å
• b: 7.4291 ± 0.0013 Å
• c: 21.345 ± 0.004 Å
• α: 90°
• β: 101.411 ± 0.005°
• γ: 90°
• Cell volume: 2764.6 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0633
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0942
• Weighted residual factors for all reflections included in the refinement: 0.1045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No