Information card for entry 7249922

Structure parameters

• Common name: tetrakis-[(μ~3~-methanolato-κ^3^O:O:O)(methanol-κO)(2-oxyacetophenone-κ^2^O,O')nickel(II)]
• Formula: C40 H56 Ni4 O16
• Calculated formula: C40 H56 Ni4 O16
• Title of publication: Ferromagnetically coupled tetranuclear Ni(ii)-2-oxy-aceto- or benzo-phenonate complexes
• Authors of publication: Haque, Imdadul; Enamullah, Mohammed; Jhumur, Nisat Taslum; Sidhu, Baldeep K.; Herbert, David E.; Haj Hassani Sohi, Takin; Havlíček, Lubomír; Nemec, Ivan; Janiak, Christoph
• Journal of publication: RSC Advances
• Year of publication: 2025
• Journal volume: 15
• Journal issue: 6
• Pages of publication: 4250 - 4261
• a: 19.08705 ± 0.00009 Å
• b: 15.151 ± 0.00007 Å
• c: 15.82527 ± 0.00008 Å
• α: 90°
• β: 95.2175 ± 0.0005°
• γ: 90°
• Cell volume: 4557.51 ± 0.04 ų
• Cell temperature: 298.6 ± 0.14 K
• Ambient diffraction temperature: 298.6 ± 0.14 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for significantly intense reflections: 0.0967
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No